Virtual Laboratory for Instrumental Analysis (VIA)

VIA provides various tools for multimodal measurements that complement the x-ray based techniques at PETRA III beamlines with additional analytical methods to study the chemical properties and behavior of the substances. Supplementary equipment is available for sample preparation. Our pool of instruments consists of mobile and stationary devices for application directly at the beamline (online measurements) and in the laboratory (offline measurements). VIA operates as a collaboration of beamlines and the chemistry laboratories and sample environment groups at PETRA III.

 

Available Instrumentation

The use of the equipment may be requested in conjunction with or independent of a beamtime at PETRA III. Please reach out to the indicated contact person for information on availability and support.

 

Mobile devices for online and offline measurements

Suitable for in situ and operando experiments probing the sample simultaneously with the x-ray beam.

UV/Vis Setup

Avantes AVASPEC-ULS2048L

Features:
  • wavelength range 300 nm - 1100 nm
  • transmission and reflection geometry
  • dual channel spectrometer
  • Deuterium-Halogen light source (AVALIGHT-DHC)
Software: AVASOFT-FULL, Spectrometer Software version 8
Location: Bldg. 25b, preparation room beamlines P07/P21.1
Contact: Marina Sturm
 
UV-Vis setup from Avantes (left) with sample stage for fiber optics (right).
www.avantes.com

 
Mass spectrometer for gas phase analysis (available upon request in 2022)

Hiden HPR-20 R&D

Features:
  • 200 amu mass range
  • heated quartz lined capillary sampling line (2 m)
  • flow rate options from 1 atm cc/min to 20 atm cc/min possible
  • triple filter
  • twin capillary inlet
Software: MASsoft Professional & QGA FT
Location: Bldg. 48f, beamlines P07/P21.1
Contact: Marina Sturm
 
 
 
 
 
 
 
 
 
 
 
 
Mass spectrometer from Hiden.
 www.hidenanalytical.com

 

 

Stationary devices for offline measurements

Suitable for analysis of the sample in the lab prior or subsequent to the x-ray experiment.

MicroCal Differential Scanning Calorimeter (DSC)

Malvern Panalytical MicroCal PEAQ-DSC

Features:
  • 130 μL working cell volume
  • 2°C to 80°C temperature range
Software: MicroCal PEAQ-DSC
Location: Bldg. 47c, operated with P08
Bookable via DOOR
Device responsible: Chen Shen (P08)
Contact: Marina Sturm