HAXPES Spectrometer

P09 Hard X-ray Photoelectron Spectrometer

SPECS Phoibos 225HV with mounted pre-lens.

P09 Hard X-ray Photoelectron Spectrometer

Manipulator head with 4-contact sample holder compartment.

P09 Hard X-ray Photoelectron Spectrometer

Side view of the sample holder mounted onto the manipulator.

The P22 experimental hutch hosts several XPS instruments. The work horse setup is a high-resolution Hard X-ray Photoelectron Spectroscopy (HAXPES) instrument.

Photoelectrons with up to 10.5 keV kinetic energy can be measured in different experimental geometries by means of a SPECS Phoibos 225 HV hemispherical analyser with a delayline detector. For angle-resolved studies or high-transmission requirements, an optional wide angle lens (+- 30 degrees acceptance) can be adapted to the analyzer.

The analysis chamber is equipped with a custom made high-precision fully motorised OMICRON 5-axis manipulator with LHe cooling. The instrument is mounted on a motorised high-precision XZ-platform consisting of a monolithic granite support which is adjustable in height and can be translated transversely relative to the incoming X-ray beam with very high precision.

HAXPES instrument parameters

Electron spectrometer

SPECS Phoibos 225HV
wide angle lens option (+- 30 deg)

Manipulator

Omicron 5-axis
integrated He-cryostat

Sample temperature range

45 - 400K

Electron Energy range:

0 - 10.5 keV

Total Energy Resolution:

typ. 100 - 400 meV

Photoelectron references spectra

P09 Hard X-ray Photoelectron Spectrometer
P09 Hard X-ray Photoelectron Spectrometer
P09 Hard X-ray Photoelectron Spectrometer
ErUM-Pro

The BMBF funded the projects 05K19UM2/ 05K19WW1HarMomMic Johannes Gutenberg-Universität Mainz/Julius-Maximilians-Universität Würzburg titled "ToF-HAXPES: Implementierung einer Flugzeit-HAXPES Anlage mit Spinfilter-Option an Beamline P22 (PETRA III). Teilprojekte 1/2" (G. Schönhense/R. Claessen)