P64 - X-Ray Absorption Spectroscopy
P64 is dedicated to X-Ray Absorption Spectroscopy experiments, which require high flux, like QEXAFS in the sub-second timescale, EXAFS on highly-diluted systems, and to high-resolution resonant x-ray emission spectroscopy. The energy range covers 4-45keV.
CONTACT |
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GENERAL SPECIFICATIONS
techniques available | |
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photon source
|
undulator
|
period
number of periods
max power
|
|
source brilliance
|
10 18 ph /s / 0.1% bw / mA (max. 100mA)
|
polarization available
|
linear horizontal
|
energy range
|
4 keV - 44 keV |
beamline energy resolution
|
ΔE/E = 1.4 x 10-4 resp. 0.3 x 10-4 |
max flux ON SAMPLE
|
1x1013 ph/s at 8.9 keV (calculated, tuned undulator)1x1012 ph/s at 8.9 keV (calculated, tapered undulator) |
spot size ON SAMPLE
|
150 μm x 50 μm 2 mm x 1 mm |
sample type
|
any |
OPTICS
type |
liq. N2 cooled Double Crystal Monochromator |
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available reflections |
Si111 and Si311
|
energy range |
4.9 keV - 44 keV
|
resolving power |
E/ ΔE : 1x104 ... 3x104 |
type |
Oscillating Channel-Cut Monochromator (QEXAFS) |
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available reflections |
Si111
|
energy range |
5.5keV - 24 keV
|
resolving power |
E/ ΔE : 7x103 |
type |
|
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ENDSTATION
Sample environment |
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DETECTOR(S)
Transmission
|
|
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Refraction
|
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Fluorescence
|
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Total electron yield
|
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Grazing incidence angle
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Type
|
Ion Chambers |
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energy resolution
|
none
|
count rate
|
linear up to 1013 cts/s |
Beam Size |
given by slits |
typical collection time |
50ms to 300s per EXAFS scan |
Type
|
Canberra 100 element
|
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energy resolution
|
|
count rate
|
105 Hz per element |
2theta range
|
fixed at 90° |
typical collection time
|
0.1s - 5s |
CONTROL/DATA ANALYSIS
Software type
|
Spok, Tango, Taurus |
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Data output type
|
spectra, parameters such as temp., press, etc. |
Data output
|
ASCII, HDF5, NEXUS |
Software(s) for quantitative analysis
|
Athena, Artemis, FEFF |
SUPPORT LAB
A sample preparation lab with a hood and a glove box is adjacent to the control hutch.A pellet press, a balance, a heating-plate with a magnetic stirrer, and an ultrasonic bath are available.
Please contact beamline staff for specific question, if you plan to use it, or if you require additional equipment.